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Test Sample Chromatograms
Test sample chromatograms
237
SAMPLE:
Type FPD Sample
Inj Volume 1
l
Part No. 19395•60580
COMPOSITION: 20 ng/
l
(20.0 ppm W/V) each of
1-dodecanethiol and
tributylphosphate in isooctane
Detector Type FPD
Temp 200 DEGREES C
Inlet Type PACKED
OR PURGED
PACKED
Temp 200
DEGREES C
Operating Mode N/A
Purge Time On N/A min
Purge Time Off N/A
min
Oven Temp Programmed (1 ramp)
Init Temp 110
DEGREES C
Init Time 0
min
Ramp Rate ___10
Fin Temp __170
Fin Time ____3
Range 5
COLUMN:
Part No. 19095S•100
Dimensions 5 M Length, 530 ID
Sta Phase Methyl
Silicone
1.73
.07
2.11
3.16
ZE
IF
Sulfer
Filter
START
START
IF
.07
.44
2.10
2.46
3.16
ZE
Phospho-
rus
Filter
DODECANETHIOL
TRIBUTYLPHOSPHATE
DODECANETHIOL
TRIBUTYLPHOS-
PHATE
FLOW RATES (FPD AIR MODE FLOWS)
Carrier (N2) 20 +/• 1 ml/min
Hydrogen 75 +/• 2 ml/min
Air 100 +/• 3 ml/min
Makeup (N2) 0 ml/min
Split Vent N/A ml/min
Septum Purge 1•2 ml/min
HP 5890 Test Sample Operating
Conditions
FPD Packed Column Inlet
Figure 10-13.